Chemical Laboratory: Safety Management and Instrumental Calibration Technique as per ISO 17025

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Chemical Laboratory: Safety Management and Instrumental Calibration Technique as per ISO 17025 Course
Introduction:
This program integrates an understanding of performance characteristics with an appreciation of the limitations imposed by analytical instrument design, emphasizing the interconnectedness of validation and qualification processes within quality assurance systems. The program covers a broad range of topics, focusing on key instrumental techniques such as spectrophotometry, chromatography, capillary electrophoresis, and atomic emission spectroscopy.
Case studies, exercises, and practical applications are incorporated to facilitate a comprehensive understanding of the underlying concepts associated with each technique. The program also encompasses the major operations conducted in an industrial chemical laboratory, providing insights into the equipment used, their operations, validations, calibration, and maintenance. Additionally, the program places emphasis on Standard Operating Procedures (SOP), encompassing their development, revisions, standards, and implementation. By the end of the program, participants will have gained a thorough understanding of these various concepts and techniques necessary for success in the field.
Course Objectives:
By the end of the training, participants will be able to:
- Apply in-depth knowledge and skills in the chemical laboratories including analytical instrumentation, analytical techniques, laboratory equipment, operational procedures, management style, method validation, quality and safety management systems
- Use the major analytical laboratory instruments and equipment and understanding their performance characteristics, capabilities, accuracies, reliabilities, speed and limitations including UV/VIS, flow injection, infrared spectroscopy, ion chromatography, pH probes, and gas chromatography
- Calibrate and certify various laboratory instruments and calculate the uncertainty and random error
- Impart the participant’s fundamental techniques of chemical laboratory
- Understand how to validate the analytical method
- Analyze the instrument performance characteristics which includes types and interaction between different characteristics
- Prepare and handle sample for different analytical instrumentations and extract analytes from complex matrices
- Develop and modify the laboratory standard operation procedures (SOP) and interpret the requirements of the ISO 17025 quality system
- Explain the flow of work and major concerns related to the Industrial Chemical Laboratory
- Carryout sampling and sample handling
- Increase knowledge about laboratory equipment and instruments such as mechanical measurements, chemical analysis and process analyzers
- Discuss nuclear magnetic instruments covering its theory, NMR spectroscopy, design and performance idea
- Illustrate NMR applications, multi-dimensional NMR spectroscopy and solid-state NMR spectroscopy
- Perform chemical laboratory operations and gain good skills of developing and modifying the laboratory Standard Operating Procedures (SOP)
- To understand the laboratory quality requirements and appreciate the need for a quality system according to the International Standards Organization ISO 17025 standard
- To use the international Guide to Lab Quality for accreditation standard methods
- Employ the safety and environmental requirements for chemical laboratory as per OSHA standard
Who Should Attend?
Laboratory personnel and technical staff such as chemists, analysts, chemical engineers, and anybody interested in chemical analysis, research and development, environmental studies, quality control, refineries, petrochemical plants, water and wastewater plants, hospitals and medical centers.
Course Outlines:
General Aspects of Analytical Chemistry
· Terminology in analytical chemistry,
· Chemometrics,
· Figures of merit,
· Quality assurance,
· Fundamental data including those for solubility and chemical equilibria.
· The process, apparatus, and operations of analytical chemistry;
· Fundamental calculations for analytical chemistry;
· Error and error analysis;
· Statistical analysis, evaluation, and treatment of data;
· Sampling, standardization, and calibration sets;
· Aqueous solutions and chemical equilibria;
· Classical methods of analysis including gravimetric and titrimetric methods;
Separation Methods
· Development of critical guidelines,
· Definition of terms,
· Recommendations for the operation of analytical separation methods.
· Spectrochemical methods
· Critical assessment of Spectrochemical methods of analysis involving:
· Electromagnetic radiation
· Compilation of fundamental data
Mass Spectrometric Methods for Elemental and Molecular Analysis
· Parts of a mass spectrometer (Theoretical example)
· Creating ions
· Hard ionization and soft ionization
· Inductively coupled plasma
· Other ionization techniques
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